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The Schlenk Line Survival Guide

Illustrated guides designed to help you master air and moisture-sensitive chemistry

  • The Schlenk Line
    • Stopcocks vs. Teflon Taps
    • Bubblers
    • Assembly
    • Equipment
  • Guides
    • Cycling onto the Schlenk Line
    • Cannula Transfer
    • Syringes and Sure Seals
    • Cannula Filtration
    • Removing Solvent
    • Preparing NMR Samples on a Schlenk Line
    • Removing Solvent from NMR tubes
    • Refluxing Under an Inert Atmosphere
    • Freeze-Pump-Thaw
    • Static Vacuum Distillation
    • Dynamic Vacuum Distillation
    • Filtration through Celite
    • Gloveboxes
    • Solvent Stills
  • Synthetic Procedures
    • P(SiMe₃)₃
    • Lithium Sand
    • Potassium Mirror
    • Purifying LiAlH₄
  • Schlenk Line Safety
    • Gas Cylinders
  • Tips and Tricks
    • Crystallisation
    • Cleaning
  • Resources
  • About
    • Citing and Permissions
  • Gallery
  • Contact

Tips and Tricks

Here you will find useful tips and tricks:

  • Crystallisation
  • Cleaning

MORE COMING SOON!

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© 2021. This work is licensed under a CC BY-NC-ND 4.0 license.

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It's been an exciting and productive few weeks in terms of publications! I'm most proud however of my latest work which is now online in Angewandte. This was extremely challenging synthetically and intellectually, so it's a relief to see it published! Got a few more papers in the works to round of a very successful spell 🥳
New video is now available on the Synthesis Workshop YouTube channel! Go check it out!
The recording of the latest CurrentChem episode on main-group chemistry is now on YouTube. Please go check it out!
Feeling lucky! 🍀

Illustrated Guides

  • Guides
  • The Schlenk Line
    • Stopcocks vs. Teflon Taps
    • Bubblers
    • Assembly
    • Equipment
  • Guides
    • Cycling onto the Schlenk Line
    • Cannula Transfer
    • Syringes and Sure Seals
    • Cannula Filtration
    • Removing Solvent
    • Preparing NMR Samples on a Schlenk Line
    • Removing Solvent from NMR tubes
    • Refluxing Under an Inert Atmosphere
    • Freeze-Pump-Thaw
    • Static Vacuum Distillation
    • Dynamic Vacuum Distillation
    • Filtration through Celite
    • Gloveboxes
    • Solvent Stills
  • Synthetic Procedures
    • P(SiMe₃)₃
    • Lithium Sand
    • Potassium Mirror
    • Purifying LiAlH₄
  • Schlenk Line Safety
    • Gas Cylinders
  • Tips and Tricks
    • Crystallisation
    • Cleaning
  • Resources
  • About
    • Citing and Permissions
  • Gallery
  • Contact
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