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The Schlenk Line Survival Guide

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Author The Schlenk Line Survival GuidePosted on March 10, 2019April 1, 2019Leave a comment on Guides

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Was fun to present some of my research from my post-doc at the Dalton Younger Members Event #DYME2019 #research #chemistry #science #maingroup #organometallic #inorganic #organic #phosphorus #boron #schlenkline #potd #postdoc #phd

Crystals make everything better! 🍊 #realtimechem #chemistry #science #schlenkline #orange #organic #inorganic #maingroup #organometallic #crystals #potd #lookattheblue #thanksforsharing #ikaworldwide #phd #research #postdoc

Crystallising a bulky primary phosphine from degassed EtOH ❄ The reaction is all done in one pot* starting from the aryl-bromide: 1) Lithium-halogen exchange; 2) Add PX₃; 3) Do work-up to get a solution of ArPX₂; 4) Add to LiAlH₄; 5) Horrible aqueous work-up performed under Argon which involved quenching a lot of LiAlH₄; 6) Recrystallise crude product! * I used six 1 litre schlenk flasks in total 😭 I also ran out of Et₂O so used DME instead and then threw in some hexane during the extraction to help seperate the layers! #chemistry #RealTimeChem #maingroup #science #phosphorus #organic #inorganic #organometallic #phd #lab #postdoc #research #crystals #potd #votd

Officially Dr. Borys after yesterday's PhD graduation! It's all worth it for the title and tudor bonnet 🥳 #phd #graduation #chemistry #kentgrads

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The Schlenk Line
Guides
Synthetic Procedures
Schlenk Line Safety
About
Contact

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